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Chemical Reaction Lab Instruments

Our product range includes a wide range of coiled tube isothermal plug flow reactor, condensation polymerization reactor, continuously stirred tank reactor, recycled bed reactor, combined flow reactor and spining basket reactor.

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Isothermal Plug Flow Reactor (Coiled Tube Type )

In an ideal Plug Flow Reactor {PFTP} there is no mixing in the direction of flow and complete mixing perpendicular to direction of flow. Concentration of reactants varies along the length of reactor but not in radial direction. In case of a coil turbulence is introduced due to frequent change in direction of flow and presence of secondary flow, so a higher value of reaction rate constant is expected in coil tube type plug flow reactor. This set-up is used to study a non-catalytic homogeneous reaction under isothermal condition.

The set up consists of two feed tanks through which two reactants are fed to the reactor. Rotameters are provided to measure the individual flow of Chemicals. The flow rate can be adjusted by operating the needle valves provided on respective Rotameter. The magnetic drive pump is used for circulation of feed. It is a helical coil tube type reactor. Reactants enter at lower end coming out of the top of coil from where samples are collected for analysis.

Experiments

· Sponification Reaction Study in straight tube Plug Flow Reactor.

· To determine Reaction Rate Constant

Utilities Required

 

· Water Supply & Drain


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    Condensation Polymerization Reactor:-Condensation Polymerization kettle is used to carry out a condensation polymerization reaction under batch condition. Polymerization reaction can be acid catalyzed or self-catalyzed. The set-up can be used to measure the extent of reaction &.also the reaction rate constant. The set-up consists of jacketed type SS reactor fitted with variable speed agitator & baffles. Reactor is fitted with Nichrome wire heaters and digital temperature controller controls temperature. Metered quantity of nitrogen gas from a cylinder, allowed entering, in the reactor. Set-up is complete &. self-contained with sampling ports. The top cover can be removed for cleaning purpose. Feed is fed from top through a funnel provided with S.S. Ball Valve. An outlet is given to Condenser fitted with a Perken’s triangle for collecting the condensate. Vapors are allowed to enter in the shell of condenser and cooling water is allowed to pass through the tube and condensate is collected.

    Experiments

    · To determine the kinetic parameters of a Condensation polymerization reaction between Pthalic acid and Hexamethylene diamine with &.without acid catalyst

    Utilities Required

    · Water supply and drain

    · Electricity-I.5kw, Single

    · Space 0.7m x 0.7m x 1.0m

     

     


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    Continuously Stirred Tank Reactor

    In an ideal CSTR the contents in reactor are well mixed and have uniform composition throughout. Thus the exit stream has the same, composition as the fluid within the reactor. This type of reactor is known as mixed flow reactor. This set-up is used to study a non-catalytic homogeneous second order liquid phase reaction under ambient condition.

    The set up consists of two feed tanks through which two reactants are fed to the reactor. Rotameters are provided to measure the individual flow of Chemicals. The flow rate can be adjusted by operating the needle valves provided on respective Rotameter. The magnetic drive pump is used for circulation of feed. The CSTR is fitted with stirrer for proper mixing. From top outlet of it samples are collected for analysis

    Experiments :

    · Sponification Reactor studies in CSTR

    · To determine the Reaction Rate Constant

    Features :

    · Continuous operation

    · Superb Painted structure

    · Simple to operate & maintain

    · Compact & stand alone set up

    · Soundless Stirrers

    Utilities Required :

    · Water Supply & Drain

    · Electricity Supply: 1 Phase, 220 V AC, 0.5 kW


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    Recycled Bed Reactor

    We are among the topmost manufacturers, suppliers and exporters of high quality Packed Bed Reactor. This apparatus is commonly used for the studying of liquids in various packed bed arrangements. The offered apparatus also undergoes various in-house quality testing procedures before being dispatched for the customer’s end.

    Specification:

    • Compressed Air Supply at 2 Bar, 2.5 CFM
    • Water Supply and Drain
    • Electricity 500 watts, 220 V, 1 Phase
    • Floor Area 0.75 m x 0.75 m

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    Combined Flow Reactor

    In a Combined Flow Reactor, the contents are passed through two types of Reactors PFR and CSTR, connected in series. This set-up is used to study a non-catalytic homogeneous second order liquid phase reaction under ambient condition. The set up consists of two feed tanks through which two reactants are fed to the reactors. Rotameters are provided to measure the individual flow of Chemicals. The flow rate can be adjusted by operating the needle valves provided on respective Rotameter. The magnetic drive pump is used for circulation of feed. Pressure Regulator, Pressure Gauge and Safety Valve are fitted in the compressed air line. The Reactants enter at lower end of helical coil tube type reactor coming out of the top of coil again entering to the CSTR which is fitted with stirrer for proper mixing. Arrangement is made for sampling from both the reactors. From top outlet of PFR and CSTR samples are collected for analysis.

    Experiments:

    · Sponification Reactor studies in CSTR/PFR/Combined Reactor.

    · To determine the Reaction Rate Constant

    Utilities Required:

    · Compressed Air supply at 2 Bar, 0.5 CFM

    · Water Supply & Drain
    · Electricity Supply: 1 Phase, 220 V AC, 0.5 kW


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    These Storage Boxes, made of Polypropylene, prove to be an excellent option for storage of different powdered reagents & other material in the laboratory. Square shape of these boxes halp in saving shelf space. Available in three different sizes, these boxes have polypropylene caps, are autoclavable, provide good chemical resistance & heavy duty service.

    Material :Polypropylene



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      Description:-

      A batch reactor is a closed system with no input and output streams. A batch reactor can operate under conditions like Isothermal (Temperature of Reaction Mass remains constant), Perfectly mixed (composition of reaction mixture is uniform throughout), and constant volume (volume of the reaction mixture within the reactor remains constant, there is no appreciable change in the density of reaction mass). This set-up is used to study a non-catalytic homogeneous reaction under isothermal condition. The set up consists of a Reactor fitted in a constant temperature water bath. One stirrer is fitted for mixing the reactants in reactor and other is fitted in a water bath to keep the uniform temperature throughout in the bath. The temperature of the bath can be maintained from ambient to 90C with the help of Digital Temperature indicator Cum Controller. Samples can be taken out with the help of a sampling pipette.

      Experimentation:-

      • To study the progress of a Chemicals reaction and determine the kinetic parameters.
      • To determine the effect of temperature on Reaction Rate Constant.

      Specifications:

      • Determine: kinetic parameters
      • Determine Effect of temperature on Reaction Rate Constant.
      • Brand: Atico
       

       


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        Description:-

        Axial diffusion and dispersion of fluid in packed beds are important for design and operation of separation equipment and Chemicals reactors. The tracer technique, the most widely used method for the study of axial dispersion. In stimulus response experimentation, we perturb the system using pulse input of tracer and then see how the system reacts or responds to this stimulus. The analysis of the response gives the desired information about the system. The setup consists of a glass column packed with Rasching Rings and one feed tank. Water is fed to the reactor through liquid distributor, fitted at the bottom of the column. Rota meter is provided to measure the flow of water. The flow rate can be adjusted by operating the needle valve provided on Rota meter. For understanding the R.T.D. characteristics, a special arrangement to inject tracer into the lower end of reactor, using a syringe, is provided. Samples can be taken periodically from the top outlet of reactor. Pressure Regulator & Pressure Gauge are fitted in the compressed air line.

        Specifications: 

        • Type: Laboratory Equipment 
        • Brand: Atico
        • To plot RTD curve for Packed Bed Reactor

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        Plug Waft Reactor (Straight Tube Type)

        In a great Plug Glide Reactor (PFTR) there’s no mixing within the path of go with the flow and full mixing perpendicular to course of float. Focus of reactants varies alongside the size of reactor however no longer in radial course: This set-up is used to review a non-catalytic homogeneous response underneath ambient situation.

        The arrange includes two feed tanks in which two reactants are fed to the reactor. Rotameters are equipped to measure the person glide of Chemical substances. The go with the flow fee will also be adjusted by means of working the needle valves equipped on respective Rotameter. The magnetic force pump is used for circulation of feed. A straight tube kind reactor stored horizontally and inclined upward at outlet from the place samples are gathered for diagnosis

        Experiments

        • Sponification Response Learn about in straight tube Plug Go with the flow Reactor.
        • To resolve Response Fee Consistent

        Utilities Required

        • Water Provide & Drain
          Devices, Laboratory Glassware and Chemical substances required for prognosis as per the device adopted

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        Description:-

        An adiabatic batch reactor is a closed system with no input and output streams. This reactor is operated under conditions like adiabatic (Temperature of Reaction Mass keep on changing), Perfectly mixed (composition of reaction mixture is uniform throughout), and constant volume (volume of the reaction mixture within the reactor remains constant, there is no appreciable change in the density of reaction mass). This set-up is used to study a catalytic homogeneous reaction under adiabatic condition. The set-up consists of a Dewar flask of capacity 1 lit. fitted with a stirrer. The flask is double insulated by ceramic wool insulation. Temp. is measured by digital temp indicator. The whole setup is mounted on a rigid M.S. frame.

        Experimentation:-

        • To study the decomposition of Hydrogen Peroxide with water in presence of an Iodide catalyst.
        • To predict the degree of conversion from time-temperature data.

         


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        Kinetics Of Dissolution Of Benzoic Acid

        The setup consists of a Reactor in which solid cylinder of Benzoic Acid is placed and water is stirred by means of a variable speed mixer. Baffles are also provided. The Reactor is made of Stainless Steel. A Peltilizer is provided to make the solid cylinder of size 1″ diameter and 2″ height of Benzoic Acid

        Experiment:

        • To study the Kinetics of dissolution of Benzoic Acid

        Utilities Required:

        • Water Supply & Drain
          Electricity Supply: 1 Phase, 220 V AC, 0.5 kW.

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        In an ideal CSTR (Le. an ideal steady state flow reactor) the contents in reactor are well mixed and have uniform composition throughout. Thus the exit stream has the same composition as the fluid within the reactor. This type of reactor is known as mixed flow reactor. This set-up is used to study a non-catalytic homogeneous second order liquid phase reaction under isothermal condition.

        The set up consists of two feed tanks through which two reactants are fed to the reactor. Rotameters are provided to measure the individual flow of Chemicals. The flow rate can be adjusted by operating the needle valves provided on respective Rotameter. The magnetic drive pump is used for circulation of feed. The CSTR is fitted with stirrer for proper mixing. From top outlet of it samples are collected for analysis. Constant temperature water bath arrangement is provided to conduct the experiment at various temperatures.

        Experiments:

        • Sponification Reaction study in Isothermal CSTR
        • To determine the Reaction Rate Constant and effect of temperature on it

        Utilities Required:

        • Water Supply & Drain
        • Electricity Supply: I Phase, 220VAC, 1.5kW.

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        Cascade CSTR Specification:-

        In an ideal CSTR (i.e. an ideal steady state flow reactor) the contents in reactor. This set-up is used to study a non-catalytic homogeneous second order liquid phase reaction under ambient condition.

        The setup consists of three CSTR arranged in series and two feed tanks through which two reactants are fed to the reactor. Rotameters are provided to measure the individual flow of Chemicals. The flow rate can be adjusted by operating the needle valves provided on respective Rotameter. The magnetic drive pump is used for circulation of feed. Reactants from feed tanks enter in the first CSTR and are passed to second CSTR and so on. For analysis samples are collected from different ports provided.

        Experiments:

        • To study the performance of Cascade of three equal volumes CSTR’s in series for the specification of a reaction.
        • To draw the performance chart for the reactor system and evaluate the reaction rate constant at ambient condition

         

        Utilities Required:

        • Water Supply & Drain
        • Electricity Supply: 1Phase, 220V AC, 0.5 kW

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        Vapor Liquid Equilibrium Apparatus

        Specifications:

        • Tidal volume range (V t): 0 mL to 1,500 mL
        • Patient airway pressure range: -2kPa - 10kPa
        • Input voltage: 100-240V AC
          Frequency: 50/60Hz

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          Isothermal Semi-Batch Reactor

          An isothermal semi-batch reactor is a semi-closed device with one enter circulation. It’s operated below prerequisites like Isothermal (Temperature of Response Mass continues to be consistent) and completely blended (composition of response combination is uniform all the way through).

          This set-up is used to review a non-catalytic homogeneous response underneath isothermal situation. The arrange contains a Reactor geared up in a continuing temperature water tub. Earlier than beginning the response the reactor charged with the measured amount of 1 reactant. From a feed tank, any other reactant is fed to the reactor. The usage of a sampling pipette samples may also be taken out for diagnosis after the mounted interval. Rotameter is supplied to measure the go with the flow of Chemical substances. The magnetic power pump is used for circulation of feed. One stirrer is equipped for mixing the reactants in reactor and different is equipped with water tub to maintain the uniform temperature right through within the tub. The temperature of tub will also be maintained from ambient to 70C with the lend a hand of Digital Temperature indicator Cum Controller

          Experiments

          • To review a 2nd order saponification response in a Semi-Batch Reactor
          • To decide the Response Fee Consistent

          Specifications

          • Use: Water Provide & Drain
          • Electrical energy: 1.5kw, Single
          • Type: Semi-Closed
          • Brand: Atico

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            Hydrodynamics of Trickle Bed

            Tile set-up consists of a glass column. Arrangement is made for changing the glass column conveniently and filling it with any type of packing required. Air from a regulated pressure vessel passes through a sparger and allowed to enter in the column at the top. Liquid is feed from a tank, fitted with a pump and is distributed at the top of a column using a spray nozzle. Set-up is fully accompanied with manometers required. Solenoid valves are provided in the feed line at the top of column for instant release and close. The flow rate can be adjusted by operating the valves provided in respective line.

            Experiments:

            · To determine Hydrodynamics of a Trickle Bed Reactor involving the measurement of pressure drop, hold-up & flow regime

            Utilities Required:

            · Compressed air at 4 Bar

            · Water supply and drain
            · Electricity-0.5kw, Single


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            The setup consists of a glass column packed with Rasching Rings. Liquid is fed to the reactor through liquid distributor, fitted at the bottom of the column. Rota meter is provided to measure the flow. The flow rate can be adjusted by operating the needle valve provided on Rota meter. For understanding the R.T.D. characteristics, a special arrangement to inject tracer into the lower end of reactor (for liquid and gas both) is provided. Samples can be taken periodically from the top outlet of reactor

            Experiments

            • To plot RTD curve for Plug Flow Reactor
            • To determine the Dispersion No

            Utilities Required

            • Water Supply & Drain
            • Instruments, Laboratory Glassware and Chemicals required for analysis as per the system adopted

            Specifications

            • Material: Stainless steel 
            • Brand: Atico 
            • Usage: To determine the dispersion
             

             


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            Advanced Technocracy Inc.

            Kunal Chopra (CEO)
            ATICO House, 5309 Grain Market, Near B. D. Senior Secondary School Aticoindia@gmail.com
            Ambala - 133001
            Haryana, India
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